Intergranular Corrosion (IGC) Testing Services

Discover the world of intergranular corrosion (IGC) testing services and how important it is to protect the integrity of materials.

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    Intergranular Corrosion (IGC) Testing Services

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    Precision-driven testing for dimensional accuracy and compliance

    • Overview
    • Scope, Applications, and Benefits
    • Test Process
    • Specifications
    • Instrumentation
    • Results and Deliverables

    Overview

    Testing for intergranular corrosion (IGC) assesses the susceptibility of metallic materials, especially nickel-based alloys and stainless steels, to corrosion at grain boundaries. This type of corrosion occurs when the grain boundary regions differ chemically from the bulk material, usually due to carbide precipitation, sensitisation, incorrect heat treatment, or welding.

    IGC can significantly impair structural integrity and mechanical strength without causing noticeable surface damage. Therefore, in sectors including oil and gas, chemical processing, power generation, and aerospace, standardised IGC testing is crucial for quality assurance, material certification, weld assessment, and failure analysis. Manufacturers can avoid early failures and ensure long-term material performance with IGC testing services, which provide standardised, trustworthy assessments using globally accepted techniques.

    Scope, Applications, and Benefits

    Scope

    IGC testing defines methods to determine the susceptibility of stainless steels and corrosion-resistant alloys to grain boundary attack under controlled chemical environments. Standards such as ASTM A262 (for austenitic stainless steels), ASTM A923 (for duplex stainless steels), and ASTM G28 (for nickel alloys) provide procedures to assess sensitization and intergranular attack through chemical exposure and metallographic examination.

    Applications

    • Material qualification for corrosion-resistant alloys
    • Weld procedure qualification and heat treatment validation
    • Quality control of stainless steel components
    • Failure analysis of corroded parts
    • Verification of solution annealing effectiveness
    • Assessment of sensitization after fabrication

    Benefits

    • Detect susceptibility to intergranular attack
    • Ensure compliance with ASTM and industry specifications
    • Validate proper heat treatment and welding procedures
    • Prevent unexpected material failure in corrosive environments
    • Support certification and regulatory requirements
    • Enhance the reliability of critical components

    Test Process

    Specimen Preparation & Exposure

    Machine, polish, clean, and immerse specimens per ASTM under controlled conditions.

    1

    Mechanical or Weight Loss Evaluation

    Perform bend tests (where applicable) to detect grain boundary cracking or measure mass loss to determine corrosion rate.

    2

    Metallographic Examination

    Prepare cross-sections and examine under an optical microscope to assess intergranular attack depth and morphology.

    3

    Interpretation & Reporting

    Classify the material as acceptable or susceptible based on the relevant standard acceptance criteria and issue a detailed report.

    4

    Technical Specifications

    ParameterDetails
    Material TypesAustenitic SS, Duplex SS, Nickel Alloys
    Test EnvironmentSpecific acid solutions per standard requirement
    Temperature RangeTypically, boiling conditions depending on the method
    Exposure Duration15 minutes to 120 hours (depending on practice)
    Evaluation MethodMicroscopic examination, bend test, or weight loss measurement

    Instrumentation Used for Testing

    • Boiling test apparatus with temperature control
    • Acid-resistant test vessels and condensers
    • Precision analytical balance for weight loss measurements
    • Metallographic sample preparation equipment (cutting, mounting, polishing)
    • Optical microscope for grain boundary evaluation
    • Digital imaging systems for documentation
    • Fume hood and chemical safety systems

    Results and Deliverables

    • Pass/Fail Classification as per applicable ASTM standard
    • Degree of Intergranular Attack (IGA) measurement
    • Corrosion Rate (when applicable)
    • Microstructural images showing the grain boundary condition
    • Bend test observations (cracking or fissures)
    • Detailed test report including test method, exposure conditions, and compliance statement

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