ASTM E1613 Determination of Lead by Inductively Coupled Plasma Atomic Emission Spectrometry
The test method ASTM E1613 is for extracted or digested samples taken during the assessment, management, or abatement of lead risks in buildings, structures, or other sites. The lead analysis of sample extracts or digestates is covered by this test procedure. The final results of this method are displayed keeping in view the international standards and inch-pound units.
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- Overview
- Scope, Applications, and Benefits
- Test Process
- Specifications
- Instrumentation
- Results and Deliverables
Overview
ASTM E1613 is a standard test method for determining the lead content of digested samples, used for lead hazard abatement in buildings. This test method is equally important for assessing and managing lead hazards. The different techniques used include “Inductively Coupled Plasma Atomic Emission Spectrometry (ICP – AES), Graphite Furnace Atomic Absorption Spectrometry (GFAAS) or Flame Atomic Absorption Spectrometry (FAAS).
Scope, Applications, and Benefits
Scope
ASTM E1613 is a standardized testing procedure for quantifying lead in extracted or digested environmental materials (e.g., paint, soil, dust, airborne particulates) utilizing instrumental analytical methodologies such as:
- ICP-AES, or Inductively Coupled Plasma Atomic Emission Spectrometry,
- FAAS, or flame atomic absorption spectroscopy, and
- Atomic Absorption Spectrometry in Graphite Furnaces (GFAAS).
It can be used for laboratory accreditation or certification and has provisions for sample analysis and quality assurance/control.
Applications
- Lead analysis in soil, dust, and paint samples
- Environmental contamination assessment
- Lead hazard and abatement evaluation
- Occupational and industrial exposure monitoring
- Regulatory compliance and validation testing
Benefits
- Accurate quantification of lead at trace levels
- Supports multiple analytical techniques (ICP-AES, FAAS, GFAAS)
- Standardized QA/QC improves result reliability
- Suitable for accredited and certified laboratories
- Applicable to multiple environmental sample types
Testing Process
Sample Collection
Collect representative environmental samples using approved methods.
1Sample Preparation
Dry, homogenize, and weigh samples to ensure consistency.
2Data Calculation
Calculate lead concentration with appropriate corrections.
3Reporting
Document results, detection limits, and QA/QC details.
4Technical Specifications
| Parameter | Details |
|---|---|
| Sample Matrices | Soil, dust, paint, airborne particulate |
| Sample Preparation | Acid extraction or digestion |
| Analytical Techniques | ICP-AES, FAAS, GFAAS |
| Quality Control | Blanks, duplicates, spikes, control samples |
| Output | Lead concentration in mass per unit sample |
| Compliance Use | Environmental testing and laboratory accreditation |
Instrumentation Used
- Inductively Coupled Plasma–Atomic Emission Spectrometer (ICP-AES)
- Radiofrequency (RF) generator and plasma torch
- Nebulizer and spray chamber
- Sample introduction system (peristaltic pump)
- High-purity argon gas supply
- Calibration standards and reference materials
- Data acquisition and analysis software
Results and Deliverables
- Accurately determines lead (Pb) concentration in tested samples
- Confirms material quality and suitability based on lead content
- Supports the durability and safety evaluation of lead-containing specimens
- Enables classification of samples for commercial and regulatory use
- Provides reproducible and reliable data under controlled QA/QC conditions
- Assists laboratories in validating compliance with environmental standards
Frequently Asked Questions
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