ASTM D3720: Titanium Dioxide Anatase Rutile XRD Testing Services
The ratio of anatase to rutile in titanium dioxide pigments is determined using ASTM D3720 procedure. The procedure can also be used to make pigment blends and colored coatings with titanium dioxide. The SI units are to be taken as standard.

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- Overview
- Scope, Applications, and Benefits
- Test Process
- Specifications
- Instrumentation
- Results and Deliverables
What Is ASTM D3720 Titanium Dioxide Anatase Rutile XRD?
ASTM D3720 determines the ratio of anatase to rutile phases in titanium dioxide pigments using X-ray diffraction (XRD). This method quantifies crystalline composition, which directly influences pigment properties such as brightness, opacity, and durability.
This test is essential for quality control and product consistency in pigment manufacturing. It enables precise phase identification and quantification, helping ensure pigments meet performance requirements for coatings, plastics, and other applications.
Applications and Benefits of ASTM D3720 Titanium Dioxide Anatase Rutile XRD Testing
Scope
ASTM D3720 defines a standardized XRD method for determining the relative proportions of anatase and rutile phases in titanium dioxide pigments.
- Applicable to titanium dioxide pigments
- Determines anatase-to-rutile ratio
- Uses X-ray diffraction analysis
- Provides quantitative phase composition
- Suitable for quality control and research
- Supports material identification and comparison
- Ensures compliance with pigment specifications
Applications
- Paints and coatings
- Plastics and polymers
- Printing inks
- Pigment manufacturing
- Material quality control
Benefits
- Provides accurate phase composition analysis
- Ensures consistent pigment quality
- Supports performance optimization
- Enables comparison between pigment grades
- Improves product reliability
Our ASTM D3720 Testing Procedure
Sample Preparation
Pigment sample is finely prepared and mounted for XRD analysis.
1XRD Measurement
Sample is exposed to X-rays to obtain diffraction patterns.
2Peak Identification
Anatase and rutile peaks are identified from diffraction data.
3Ratio Calculation
Relative peak intensities are used to calculate phase ratio.
4ASTM D3720 Test Parameters and Requirements
| Parameter | Details |
|---|---|
| Material Type | Titanium dioxide pigments |
| Method | X-ray diffraction (XRD) |
| Measurement | Anatase-to-rutile ratio |
| Output | Phase composition percentage |
| Units | Relative percentage (%) |
| Relative percentage (%) | Powder |
| Analysis | Diffraction peak intensity |
- X-ray diffractometer (XRD)
- Sample holder and preparation tools
- Data analysis software
- Calibration standards
- Laboratory balance
Equipment and Instrumentation Used for ASTM D3720 Testing
What You Receive: Test Report, Data, and Certification
- Anatase and rutile percentage
- Diffraction pattern data
- Phase identification report
- Test conditions and observations
- Compliance statement with ASTM D3720
ASTM D3720 Titanium Dioxide Anatase Rutile XRD FAQs
ASTM D3720 is used to determine the ratio of anatase to rutile phases in titanium dioxide pigments using X-ray diffraction. It ensures pigment quality, consistency, and performance by accurately identifying crystalline composition for various industrial applications.
The ratio affects optical and durability properties. Rutile provides better opacity and weather resistance, while anatase offers higher brightness. Controlling the ratio ensures pigments meet specific performance requirements in coatings, plastics, and other products.
XRD identifies crystalline phases by analyzing diffraction patterns produced when X-rays interact with the material. Each phase has unique peaks, allowing precise identification and quantification of anatase and rutile components.
Factors include sample homogeneity, instrument calibration, measurement conditions, and data analysis methods. Proper control ensures reliable results.
Anatase offers higher brightness and whiteness but lower durability compared to rutile, making it suitable for indoor or less demanding applications.
Why Choose Infinita Lab for Titanium Dioxide Anatase Rutile XRD Testing?
At the core of this breadth is our network of 2,000+ accredited laboratories across the USA, offering access to over 10,000 testing methods and analytical services. From advanced materials characterization (SEM, TEM, RBS, XPS) to mechanical, chemical, environmental, biological, and standardized ASTM/ISO-compliant testing, we deliver unmatched flexibility, specialization, and scale. You are never limited by geography, facility, or methodology — Infinita Lab connects you to the right expertise and testing solution, every time.
Looking for an Accredited Partner for ASTM D3720 Titanium Dioxide Anatase Rutile XRD Testing?
Send query us at hello@infinitalab.com or call us at (888) 878-3090 to learn more about our services and how we can support you.

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