ASTM D7599 Determination of Ethanol Amines in Water by Liquid Chromatography

ASTM D7599 test method uses the techniques of liquid chromatography and single reaction monitoring mass spectrometry for the quantitative and qualitative determination of diethanolamine, triethanolamine, N-methyldiethanolamine, and N-methyl diethanolamine in surface water. The final results of this method are expressed in SI units.

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    Scope:

    ASTM D7599 test method deals with the determination of ethanolamines in surface water which serve as chemical weapons. There can be varied uses of these chemical weapons, such as their application in the production of adhesives, agricultural products, cement grinding aids, detergents, various chemical products, polishes, pesticides, and pharmaceuticals. These ethanolamines are biodegradable and can thus be easily dissolved in water. This test method determines their applications, properties, and significance.

    Procedure:

    The ASTM D7599 test method is aimed at determining the performance of various ethanolamines. For this purpose, the samples are taken and treated in the lab at a specific temperature range. There the samples are filtered and analyzed, and recognized by their retention time. The final report is issued after carefully determining the concentration of different ethanolamines in the sample. 

    Video 01: Introduction to liquid chromatography

    Specimen size:

    Specimen size must be in accordance with the requirements. The ASTM D7599 test method requires about 25 mL of the sample solution.

    Data:

    The percent recovery of the spike (P) is calculated and provided.

    Conclusion:

    ASTM D7599 test method deals with the determination of ethanolamines in surface water which serve as chemical weapons.

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